不同采后浸泡方式对豇豆农药残留的去除效果

Effects of different postharvest soaking methods on the removal of pesticide residues in cowpea

  • 摘要: 【目的】研究不同采后浸泡方式对豇豆中农药残留去除效果的影响,为豇豆质量安全风险管理及膳食风险评估提供理论基础。【方法】以田间喷施毒死蜱、水胺硫磷、氧乐果和丁硫克百威的豇豆为研究对象,分别于喷药后第1、3、5和14 d进行采摘,然后采用常温清水、冰水和1%冰碱水均分别浸泡5、10和15 min的方式进行处理,以未经浸泡处理为对照,对豇豆中毒死蜱、氧乐果、丁硫克百威和水胺硫磷残留量进行检测,分析不同采后浸泡方式对豇豆中农药残留的去除效果。【结果】通过清水、冰水和1%冰碱水浸泡豇豆均能在一定程度上降低毒死蜱、氧乐果、丁硫克百威和水胺硫磷的残留量;其中,喷施丁硫克百威和水胺硫磷后第5 d采摘于1%冰碱水浸泡15 min的洗脱效果最佳,去除率分别为69.37%和49.67%;喷施毒死蜱后第5 d采摘于1%冰碱水浸泡10 min的洗脱效果最佳,去除率为44.94%;喷施氧乐果后第1 d采摘于1%冰碱水浸泡5 min的洗脱效果最佳,去除率为53.83%。喷药后第5 d,经3种浸泡方式处理的豇豆仅丁硫克百威的最大农药残留量符合国家限量值标准(≤0.01 mg/kg)。【结论】毒死蜱、氧乐果和水胺硫磷在喷药5 d内,通过常温清水、冰水和1%冰碱水浸泡方式均无法达到国家限量标准,我国实行高毒农药在豇豆中的禁限用十分必要。

     

    Abstract: 【Objective】To study the effects of different postharvest soaking methods on the removal of pesticide residues in cowpea, which could provide theoretical basis for cowpea quality and safety risk management and dietary risk assessment. 【Method】Cowpeas sprayed with chlorpyrifos,isocarbopho,omethoate and carbosulfan were harvested on the 1st, 3rd, 5th and 14th d after spraying, and then soaked in room temperature water, ice water and 1% ice alkali water for 5,10 and 15 min respectively. Without soaking treatment was as control. The residues of chlorpyrifos,omethoate, carbosulfan and isocarbopho in cowpea were detected, and the removal effects of different postharvest soaking methods on pesticide residues in cowpea were analyzed.【Result】Soaking cowpea in water, ice water and 1% ice alkali water could reduce the residues of cchlorpyrifos,omethoate,isocarbopho and carbosulfan to a certain extent. The best elution effect was obtained on the 5th d after carbofuran and isocarbopho were sprayed in 1% ice alkali water for 15 min, and the removal rates were 69.37% and 49.67% respectively. On the 5th d after spraying chlorpyrifos, the picked cowpeas were soaked in 1% ice alkali water for 10 min, and the removal rate was 44.94%. On the 1st d after spraying omethoate, the best elution effect was obtained by soaking in 1% ice alkali water for 5 min, and the removal rate was 53.83%. On the 5th d after spraying, the maximum pesticide residue of carbosulfan in cowpea treated by 3 soaking methods met the national limit value standard (≤0.01 mg/kg). 【Conclusion】Chlorpyrifos,omethoate and isocarbopho within 5 d of spraying, through room temperature water, ice water and 1% ice alkali water can not reach the national limit standard. The forbidden and restriction of higly toxic pesticides in cowpea is very necessary in China.

     

/

返回文章
返回